Glassy carbon manufacture using rapid photonic curing

نویسندگان

چکیده

Abstract Photonic curing was explored as a rapid method for producing glassy carbon coatings, reducing processing time from ~ 20 h conventional thermal down to 1 min. A resole-type thermoset polymer resin coated on steel foil used precursor, placed in nitrogen purged container and exposed high energy light (~ 27 J/cm 2 per pulse up pulses). Comparison samples were produced at 800 °C using route. For both photonic conventionally Raman spectroscopy primary peak XPS data showed sp bonded carbon, indicative of bulk carbon. This transformation evolved with increasing number pulses, therefore amount transferred the coating. The coatings resilient, highly smooth, no evidence surface defects. analysis indicated greater 3 content immediate (5–10 nm) cured compared thermally likely due local environment (temperature, atmosphere) around during conversion. ability rapidly manufacture provides new opportunities expand window applications carbons towards large-scale volume applications.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Antineoplasic Drug Methotrexate Redox Mechanism Using a Glassy Carbon Electrode

Methotrexate (MTX) is an antimetabolite of folic acid indicated in the treatment of a variety of cancers. The electrochemical behaviour of MTX on a glassy carbon electrode was investigated. The MTX oxidation is a complex, pH-dependent, diffusion-controlled irreversible process and proceeds with the transfer of two electrons and two protons and the formation of one electroactive product, 7-hydro...

متن کامل

Electrochemical Chiral Recognition of Naproxen Using L-Cysteine/Reduced Graphene Oxide Modified Glassy Carbon Electrode

The electrochemical response of S- and R-naproxen enantiomers was investigated on L-cysteine/reduced graphene oxide modified glassy carbon electrode (L-Cys/RGO/GCE). The production of the reduced graphene oxide and L-cysteine on the surface of the glassy carbon electrode was done by using electrochemical processes. Cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) were us...

متن کامل

Cyclic voltammetry of bulk and nano manganese sulfate with Doxorubicin using glassy Carbon electrode

The cyclic voltammetry of both bulk manganese sulfate (BMS) and nano manganese sulfate (NMS) were studied using 0.1M KCl supporting electrolyte and glassy carbon working electrode. The redox behavior for both bulk (BMS) and MnSO4 (NMS) sulfate was studied voltammetrically in presence and absence of Doxorubicin (DR) using three electrodes system, silver- silver chloride (Ag/AgCl), pla...

متن کامل

Rapid Manufacture of Novel Variable Impedance Robots

Variable stiffness and variable damping can play an important role in robot movement, particularly for legged robots such as bipedal walkers. Variable impedance also introduces new control problems, since there are more degrees of freedom to control, and the resulting robot has more complex dynamics. In this paper, we introduce novel design and fabrication methodologies that are capable of prod...

متن کامل

Characterization of photonic crystal microcavities with manufacture imperfections.

The manufacture of a photonic crystal always produce deviations from the ideal case. In this paper we present a detailed analysis of the influence of the manufacture errors in the resulting electric field distribution of a photonic crystal microcavity. The electromagnetic field has been obtained from a FDTD algorithm. The results are studied by using the Principal Component Analysis method. Thi...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Journal of Materials Science

سال: 2022

ISSN: ['1573-4803', '0022-2461']

DOI: https://doi.org/10.1007/s10853-021-06648-w